9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁶-benzoyl adenine

Base Information

• Chemical Name: 9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁶-benzoyl adenine
• CAS No.: 1020068-62-5
• Molecular Formula: C₃₉H₃₄FN₅O₆
• Molecular Weight: 687.727

Synonyms:9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁶-benzoyl adenine

Chemical Property of 9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁶-benzoyl adenine

Chemical Property:

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Technology Process of 9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁶-benzoyl adenine

There total 1 articles about 9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N⁶-benzoyl adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

9-(2-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N6-benzoyl adenine (1020068-60-3) + trityl chloride (76-83-5) → 9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N6-benzoyl adenine (1020068-62-5)

Guidance literature:

With pyridine; dmap; at 60 ℃; for 12h;

DOI:10.1016/j.ejmech.2007.04.001

Reference yield: 50.0%

9-(2-O-acetyl-3-deoxy-3-fluoro-6-O-trityl-β-D-glucopyranosyl)-N6-benzoyl adenine (1020068-62-5) → 9-(3-deoxy-3-fluoro-6-O-trityl-β-D-glycero-hex-2-enopyranosyl-4-ulose)-N6-benzoyl adenine (1020068-66-9)

Guidance literature:

With dipyridinium dichromate; acetic anhydride; In dichloromethane; at 90 ℃; for 1.66667h;

DOI:10.1016/j.ejmech.2007.04.001

upstream raw materials:

9-(2-O-acetyl-3-deoxy-3-fluoro-β-D-glucopyranosyl)-N⁶-benzoyl adenine

trityl chloride

Downstream raw materials:

9-(3-deoxy-3-fluoro-6-O-trityl-β-D-glycero-hex-2-enopyranosyl-4-ulose)-N⁶-benzoyl adenine

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