C₁₇H₁₇BrN₂

Base Information

• Chemical Name: C₁₇H₁₇BrN₂
• CAS No.: 1241668-59-6
• Molecular Formula: C₁₇H₁₇BrN₂
• Molecular Weight: 329.239
• Mol file: 1241668-59-6.mol

Synonyms:C₁₇H₁₇BrN₂

Chemical Property of C₁₇H₁₇BrN₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₇BrN₂

There total 2 articles about C₁₇H₁₇BrN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-bromo-1H-indole (52415-29-9) → C17H17BrN2 (1241668-59-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 20 °C

2.1: lithium aluminium tetrahydride / 48 h / -78 - 20 °C

3.1: sodium sulfate / methanol / 12 h

3.2: 0 °C

With lithium aluminium tetrahydride; sodium sulfate; trifluoroacetic acid; In methanol; dichloromethane;

DOI:10.1002/chem.201805945

Reference yield:

3-(2-nitrovinyl)-6-bromo-1H-indole (319493-07-7) → C17H17BrN2 (1241668-59-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / 48 h / -78 - 20 °C

2.1: sodium sulfate / methanol / 12 h

2.2: 0 °C

With lithium aluminium tetrahydride; sodium sulfate; In methanol;

DOI:10.1002/chem.201805945

Reference yield: 85.0%

carbonic acid (E)-4-bromobut-2-en-1-yl methyl ester + C17H17BrN2 (1241668-59-6) → C23H25BrN2O3 (1241667-83-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja105111n

upstream raw materials:

6-bromo-1H-indole

3-(2-nitrovinyl)-6-bromo-1H-indole

Downstream raw materials:

C₂₃H₂₅BrN₂O₃