Technology Process of C52H68F3N5O27
There total 8 articles about C52H68F3N5O27 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver trifluoromethanesulfonate; tetramethylurea;
In
dichloromethane;
at 20 ℃;
for 20h;
Molecular sieve;
DOI:10.1055/s-0032-1317961
- Guidance literature:
-
Multi-step reaction with 2 steps
1: titanium(IV) bromide / dichloromethane / 3 h / 20 °C
2: silver trifluoromethanesulfonate; tetramethylurea / dichloromethane / 20 h / 20 °C / Molecular sieve
With
silver trifluoromethanesulfonate; titanium(IV) bromide; tetramethylurea;
In
dichloromethane;
DOI:10.1055/s-0032-1317961
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1,2-dichloro-ethane
2: sodium azide / dimethyl sulfoxide / 80 °C
3: sodium methylate; methanol
4: toluene-4-sulfonic acid / acetonitrile
5: pyridine
6: sodium cyanoborohydride; methanesulfonic acid / tetrahydrofuran
7: silver trifluoromethanesulfonate; tetramethylurea / dichloromethane / 20 h / 20 °C / Molecular sieve
With
pyridine; methanol; sodium azide; methanesulfonic acid; sodium methylate; silver trifluoromethanesulfonate; sodium cyanoborohydride; toluene-4-sulfonic acid; tetramethylurea;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1055/s-0032-1317961