O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

Base Information

Chemical Name:O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate
CAS No.:866145-55-3
Molecular Formula:C₁₇H₁₆ClFNO₈P
Molecular Weight:447.741
Hs Code.:

Synonyms:O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

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Chemical Property of O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

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Technology Process of O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

There total 3 articles about O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 103796-61-8
dimethyl 1-hydroxy-1-(3-nitrophenyl)methylphosphonate

: 826990-46-9
2-(2-chloro-4-fluorophenoxy)acetyl chloride

: 866145-55-3
O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

Guidance literature:: With triethylamine; In chloroform; at 2 - 20 ℃;
DOI:10.1021/jf104247w

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 866145-55-3
O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

2: triethylamine / chloroform / 2 - 20 °C

With triethylamine; In chloroform;
DOI:10.1021/jf104247w

Reference yield:

: 399-41-7
2-(2-chloro-4-fluorophenoxy)acetic acid

: 866145-55-3
O,O-dimethyl α-(2-chloro-4-fluorophenoxyacetoxy)-3-nitrobenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: triethylamine / chloroform / 2 - 20 °C

With thionyl chloride; triethylamine; In chloroform;
DOI:10.1021/jf104247w