benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

Base Information

Chemical Name:benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate
CAS No.:1557159-75-7
Molecular Formula:C₂₆H₃₅N₃O₇
Molecular Weight:501.58
Hs Code.:

Synonyms:benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

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Chemical Property of benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

Chemical Property:

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Technology Process of benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

There total 4 articles about benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1557159-80-4
C₁₈H₂₉N₃O₅

: 501-53-1,94274-21-2
benzyl chloroformate

: 1557159-75-7
benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

Guidance literature:: C₁₈H₂₉N₃O₅; benzyl chloroformate; With triethylamine; In methanol; for 1h;

With potassium carbonate; In methanol; for 1h;
DOI:10.1039/c3cc48761j

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 1557159-75-7
benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 120 °C / Dean-Stark

2.1: methanol; sodium tetrahydroborate / acetone / 0.5 h

3.1: triethylamine / methanol / 1 h

3.2: 1 h

With methanol; sodium tetrahydroborate; triethylamine; In methanol; acetone; toluene;
DOI:10.1039/c3cc48761j

Reference yield:

: 51857-17-1
tert-butyl N-(6-aminohexyl)carbamate

: 1557159-75-7
benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 120 °C / Dean-Stark

2.1: methanol; sodium tetrahydroborate / acetone / 0.5 h

3.1: triethylamine / methanol / 1 h

3.2: 1 h

With methanol; sodium tetrahydroborate; triethylamine; In methanol; acetone; toluene;
DOI:10.1039/c3cc48761j