sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

Base Information

Chemical Name:sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate
CAS No.:1377617-68-9
Molecular Formula:C₂₄H₂₁N₂O₂S₂*Na
Molecular Weight:456.565
Hs Code.:

Synonyms:sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

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Chemical Property of sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

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Technology Process of sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

There total 3 articles about sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1377617-66-7
4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzonitrile

: 1377617-68-9
sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

Guidance literature:: With sodium hydroxide; In ethanol; water; for 2h; Reflux;
DOI:10.1039/c2cc31131c

Reference yield:

: 24243-31-0
benzo[1,2-b:4,3-b’]dithiophene-4,5-quinone

: 1377617-68-9
sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 100 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 95 °C

2.2: 20 - 95 °C

3.1: sodium hydroxide / ethanol; water / 2 h / Reflux

With ammonium acetate; potassium carbonate; acetic acid; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c2cc31131c

Reference yield:

: 105-07-7
4-cyanobenzaldehyde

: 1377617-68-9
sodium 4-(1-hexyl-1H-dithieno[2',3':3,4;3'',2'':5,6]benzo[1,2-d]imidazol-2-yl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ammonium acetate; acetic acid / 100 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 95 °C

2.2: 20 - 95 °C

3.1: sodium hydroxide / ethanol; water / 2 h / Reflux

With ammonium acetate; potassium carbonate; acetic acid; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c2cc31131c