[2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine

Base Information

• Chemical Name: [2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine
• CAS No.: 115643-25-9
• Molecular Formula: C₁₉H₂₉NO
• Molecular Weight: 287.445
• Mol file: 115643-25-9.mol

Synonyms:[2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine

Chemical Property of [2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine

There total 1 articles about [2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-(3-Ethoxypropyl)-cyclohexanon (115643-24-8) + rac-methylbenzylamine (618-36-0) → [2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine (115643-25-9)

Guidance literature:

toluene-4-sulfonic acid; In toluene; for 24h; Heating;

DOI:10.1002/ardp.19883210216

Reference yield:

[2-(3-Ethoxy-propyl)-cyclohex-(E)-ylidene]-(1-phenyl-ethyl)-amine (115643-25-9) → cis-2-(3-Ethoxypropyl)-1-(N-1-phenylethyl)-aminocyclohexan + trans-2-(3-Ethoxypropyl)-1-(N-1-phenylethyl)-aminocyclohexan

Guidance literature:

With hydrogen; nickel; In ethanol; for 96h; under 3750.3 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1002/ardp.19883210216

upstream raw materials:

2-(3-Ethoxypropyl)-cyclohexanon

rac-methylbenzylamine