[Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl₂]Cl

Base Information

• Chemical Name: [Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl₂]Cl
• CAS No.: 859147-94-7
• Molecular Formula: C₁₀H₁₆Cl₂CrN₄O₄*Cl
• Molecular Weight: 414.616
• Mol file: 859147-94-7.mol

Synonyms:[Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl₂]Cl

Chemical Property of [Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl₂]Cl

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of [Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl₂]Cl

There total 1 articles about [Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl₂]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane (706780-51-0) + chromium(III) chloride (10025-73-7,16284-59-6) → [Cr(2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane)Cl2]Cl (859147-94-7)

Guidance literature:

In ethanol; hot soln. ligand in EtOH and hot soln. metal salt in EtOH were mixed together and refluxed for 4-9 h at 78°C; react. mixt. was cooled, ppt. was filtered, washed with cold EtOH, driedunder vac. over P4O10 and recrystd.; elem. anal.;

DOI:10.1016/j.saa.2004.06.060

upstream raw materials:

2,3,9,10-tetraketo-1,4,8,11-tetraazacyclotetradecane

chromium(III) chloride