4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

Base Information

Chemical Name:4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol
CAS No.:451456-45-4
Molecular Formula:C₁₃H₉ClF₃NO₃
Molecular Weight:319.668
Hs Code.:

Synonyms:4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

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Chemical Property of 4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

Chemical Property:

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Technology Process of 4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

There total 4 articles about 4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 451456-44-3
6-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-phenyl-4H-1,3,2-benzodioxaborinin

: 451456-45-4
4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/jf0116395

Reference yield:

: 69045-89-2
2-(4'-hydroxyphenoxy)-3-chloro-5-trifluoromethylpyridine

: 451456-45-4
4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / propanoic acid / benzene / 3 h / Heating

2: 82 percent / 30 percent H₂O₂ / tetrahydrofuran / 2 h / 20 °C

With dihydrogen peroxide; propionic acid; In tetrahydrofuran; benzene;
DOI:10.1021/jf0116395

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 451456-45-4
4-[(3-chloro-5-(trifluoromethyl)-2-pyridinyl)oxy]-2-(hydroxymethyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / aq. NaOH / dimethylsulfoxide

2: 57 percent / propanoic acid / benzene / 3 h / Heating

3: 82 percent / 30 percent H₂O₂ / tetrahydrofuran / 2 h / 20 °C

With sodium hydroxide; dihydrogen peroxide; propionic acid; In tetrahydrofuran; dimethyl sulfoxide; benzene;
DOI:10.1021/jf0116395