diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

Base Information

Chemical Name:diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate
CAS No.:1239876-74-4
Molecular Formula:C₃₀H₃₈N₃O₉PS
Molecular Weight:647.686
Hs Code.:

Synonyms:diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

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Chemical Property of diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

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Technology Process of diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

There total 4 articles about diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1239876-73-3
diisopropyl N-[2-benzyloxycarbonylamino-N₃-(tert-butoxycarbonyl)-3-(4-phenoxybenzenesulfonamido)propyl]carbamoylphosphonate

: 1239876-74-4
diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

Guidance literature:: diisopropyl N-[2-benzyloxycarbonylamino-N₃-(tert-butoxycarbonyl)-3-(4-phenoxybenzenesulfonamido)propyl]carbamoylphosphonate; With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With sodium hydrogencarbonate; In dichloromethane;

Reference yield:

: 83877-27-4
diisopropyl 4-nitrophenoxycarbonylphosphonoformate

: 1239876-74-4
diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 1 h / 0 - 20 °C

2.1: trifluoroacetic acid / methanol; chloroform / 7 h / 0 - 20 °C

3.1: water; ethyl acetate / 1.5 h / 0 - 20 °C

4.1: triphenylphosphine / toluene / 0.08 h / 20 °C

4.2: 12 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With triphenylphosphine; trifluoroacetic acid; In methanol; dichloromethane; chloroform; water; ethyl acetate; toluene; 4.1: |Mitsunobu Displacement / 4.2: |Mitsunobu Displacement;
DOI:10.1002/hc.21256

Reference yield:

: C₁₀H₂₃N₂O₅P

: 1239876-74-4
diisopropyl (S)-2-benzyloxycarbonylamino-3-(4-phenoxybenzenesulfonamido)propylcarbamoylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: water; ethyl acetate / 1.5 h / 0 - 20 °C

2.1: triphenylphosphine / toluene / 0.08 h / 20 °C

2.2: 12 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

With triphenylphosphine; trifluoroacetic acid; In dichloromethane; water; ethyl acetate; toluene; 2.1: |Mitsunobu Displacement / 2.2: |Mitsunobu Displacement;
DOI:10.1002/hc.21256