Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

Base Information

Chemical Name:Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate
CAS No.:153902-65-9
Molecular Formula:C₃₀H₄₂O₄Si
Molecular Weight:494.747
Hs Code.:

Synonyms:Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

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Chemical Property of Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

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Technology Process of Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

There total 3 articles about Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 15719-55-8
trimethyl(oct-1-yn-1-yl)silane

: 153902-62-6
Diethyl (2-Bromo-2-propenyl)-3-(phenyl-2-propynyl)malonate

: 153902-65-9
Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide; at 125 ℃; for 3h;
DOI:10.1016/S0040-4020(01)87263-X

Reference yield:

: 86953-47-1
Diethyl 2-(2-bromo-2-propenyl)malonate

: 153902-65-9
Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: 63 percent / NEt₃ / Cl₂Pd(PPh₃)2, n-BuLi / dimethylformamide; tetrahydrofuran / 3 h / 125 °C

With sodium hydride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)87263-X

Reference yield:

: 82490-61-7
3-phenyl-2-propyn-1-yl methanesulfonate

: 153902-65-9
Diethyl 4-Phenyl-5-(n-hexyl)-6-(trimethylsilyl)-2,2-indanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran

2: 63 percent / NEt₃ / Cl₂Pd(PPh₃)2, n-BuLi / dimethylformamide; tetrahydrofuran / 3 h / 125 °C

With sodium hydride; triethylamine; bis-triphenylphosphine-palladium(II) chloride; n-butyllithium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)87263-X