4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

Base Information

Chemical Name:4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol
CAS No.:721959-32-6
Molecular Formula:C₂₃H₂₂BrIO
Molecular Weight:521.236
Hs Code.:

Synonyms:4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

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Chemical Property of 4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

Chemical Property:

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Technology Process of 4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

There total 3 articles about 4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 624-38-4,1032416-46-8
para-diiodobenzene

: 91404-26-1
(4-tert-butylphenyl)(4-bromophenyl)methanone

: 721959-32-6
4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

Guidance literature:: para-diiodobenzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 2h;

(4-tert-butylphenyl)(4-bromophenyl)methanone; In diethyl ether; hexane; at -78 - 20 ℃; for 24h;
DOI:10.1021/ja031549b

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 721959-32-6
4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane; diethyl ether / 2 h / -78 °C

1.2: 90 percent / hexane; diethyl ether / 24 h / -78 - 20 °C

2.1: n-BuLi / hexane; diethyl ether / 2 h / -78 °C

2.2: 93 percent / hexane; diethyl ether / 24 h / -78 - 20 °C

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ja031549b

Reference yield:

: {4-(tert-butyl)phenyl}(pyrrolidin-1-yl)methanone

: 721959-32-6
4-bromo-4'-iodo-4''-tert-butyltriphenylmethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane; diethyl ether / 2 h / -78 °C

1.2: 90 percent / hexane; diethyl ether / 24 h / -78 - 20 °C

2.1: n-BuLi / hexane; diethyl ether / 2 h / -78 °C

2.2: 93 percent / hexane; diethyl ether / 24 h / -78 - 20 °C

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ja031549b