ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate

Base Information

• Chemical Name: ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate
• CAS No.: 1582767-25-6
• Molecular Formula: C₁₆H₁₉N₃O₂
• Molecular Weight: 285.346

Synonyms:ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate

Chemical Property of ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate

There total 1 articles about ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1-phenylmethyl-4-piperidone (3612-20-2) + oxalic acid diethyl ester (95-92-1) → ethyl 5-benzyl-4,5,6,7-tetrahydro-2H-pyrazolo[4,3-c]pyridine-3-carboxylate (1582767-24-5,912635-58-6) + ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate (1582767-25-6) + ethyl 5-(2-(benzylamino)ethyl)-1H-pyrazole-3-carboxylate (1582767-26-7)

Guidance literature:

1-phenylmethyl-4-piperidone; oxalic acid diethyl ester; With sodium ethanolate; In ethanol; at -10 - 20 ℃; Inert atmosphere;

With hydrazine hydrate; In ethanol; at 20 ℃; for 0.0833333h;

With pyridinium p-toluenesulfonate; In ethanol; at 20 ℃; for 6h; Reagent/catalyst;

DOI:10.1071/CH13468

Reference yield: 98.0%

ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate (1582767-25-6) → C14H14N3O2(1-)*Li(1+) (1582767-42-7)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃;

DOI:10.1071/CH13468

Reference yield: 93.0%

ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate (1582767-25-6) → C14H15N3O (1582767-34-7)

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; Inert atmosphere;

DOI:10.1071/CH13468

upstream raw materials:

1-phenylmethyl-4-piperidone

oxalic acid diethyl ester

Downstream raw materials:

C₁₄H₁₅N₃O

C₂₀H₂₈N₄

C₂₀H₂₄N₄O

C₁₉H₂₆N₄O

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1582767-25-6 ethyl 6-benzyl-4,5,6,7-tetrahydropyrazolo[1,5-c]pyrimidine-2-carboxylate

Send

Send

Metric Ton KG G Pound L ML

Send

Send