(3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

Base Information

Chemical Name:(3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene
CAS No.:142560-84-7
Molecular Formula:C₁₉H₂₃NO₃S
Molecular Weight:345.463
Hs Code.:

Synonyms:(3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

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Chemical Property of (3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

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Technology Process of (3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

There total 3 articles about (3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 129396-35-6
-1-(2-phenylpropylsulfinyl)-2-nitrocyclopentene

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 142467-47-8
(3aR,4R,7S,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

: 142560-84-7
(3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

Guidance literature:: With hydroquinone; In tetrahydrofuran; for 120h; under 6000480 Torr; Ambient temperature;
DOI:10.1016/S0957-4166(00)82293-4

Reference yield: 39.0%

: 129396-35-6
-1-(2-phenylpropylsulfinyl)-2-nitrocyclopentene

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 142467-45-6
(3aR,4R,7aS)-4-Methyl-3a-nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-indene

: 142560-84-7
(3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

Guidance literature:: With hydroquinone; In tetrahydrofuran; for 120h; under 6000480 Torr; Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00087a043

Reference yield:

: 129396-35-6
-1-(2-phenylpropylsulfinyl)-2-nitrocyclopentene

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 142467-45-6
(3aR,4R,7aS)-4-Methyl-3a-nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-indene

: 142467-47-8
(3aR,4R,7S,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

: 142560-84-7
(3aR,4S,7R,7aS)-3a-Nitro-7a-((S)-(S)-2-phenyl-propane-1-sulfinyl)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methano-indene

Guidance literature:: With hydroquinone; In dichloromethane; for 120h; under 6000480 Torr; Product distribution; Ambient temperature; other pressure; other time; other solvent; also other dienes used;
DOI:10.1021/jo00087a043