7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1⁽⁵⁾-ene-3-thione

Base Information

• Chemical Name: 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1⁽⁵⁾-ene-3-thione
• CAS No.: 473713-33-6
• Molecular Formula: C₁₇H₁₂ClNS₃
• Molecular Weight: 361.94

Synonyms:7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1⁽⁵⁾-ene-3-thione

Chemical Property of 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1⁽⁵⁾-ene-3-thione

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Technology Process of 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1⁽⁵⁾-ene-3-thione

There total 4 articles about 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1⁽⁵⁾-ene-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

dithiophosphoric acid S-[(4-chloro-phenyl)-(4-oxo-2-thioxo-3-o-tolyl-thiazolidin-5-yl)-methyl] ester O,O'-diethyl ester → 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1(5)-ene-3-thione (473713-33-6)

Guidance literature:

With sodium t-butanolate; In tert-butyl alcohol; for 4h; Heating;

Reference yield:

3-(2-methylphenyl)-2-thioxothiazolidin-4-one (23522-37-4,151797-49-8,151797-50-1,1013919-44-2,1013919-45-3) → 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1(5)-ene-3-thione (473713-33-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / 2-methyl-propan-2-ol / 3 h / Heating

2: 92 percent / t-BuONa / 2-methyl-propan-2-ol / 4 h / Heating

With sodium t-butanolate; In tert-butyl alcohol;

Reference yield:

4-chlorobenzaldehyde (104-88-1) → 7-(4-chloro-phenyl)-4-o-tolyl-2,6-dithia-4-aza-bicyclo[3.2.0]hept-1(5)-ene-3-thione (473713-33-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 86 percent / 2-methyl-propan-2-ol / 3 h / Heating

2: 92 percent / t-BuONa / 2-methyl-propan-2-ol / 4 h / Heating

With sodium t-butanolate; In tert-butyl alcohol;

upstream raw materials:

3-(2-methylphenyl)-2-thioxothiazolidin-4-one

4-chlorobenzaldehyde

5-[1-(4-Chloro-phenyl)-meth-(Z)-ylidene]-2-thioxo-3-o-tolyl-thiazolidin-4-one

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