C₂₇H₃₅N₇O₂

Base Information

Chemical Name:C₂₇H₃₅N₇O₂
CAS No.:1346243-42-2
Molecular Formula:C₂₇H₃₅N₇O₂
Molecular Weight:489.621
Hs Code.:

C<sub>27</sub>H<sub>35</sub>N<sub>7</sub>O<sub>2</sub>

Synonyms:C₂₇H₃₅N₇O₂

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Chemical Property of C₂₇H₃₅N₇O₂

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Technology Process of C₂₇H₃₅N₇O₂

There total 9 articles about C₂₇H₃₅N₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1346245-59-7
C₃₂H₄₃N₇O₄

: 1346243-42-2
C₂₇H₃₅N₇O₂

Guidance literature:: C₃₂H₄₃N₇O₄; With trifluoroacetic acid; In dichloromethane; at 10 - 20 ℃; for 18h;

With potassium carbonate; In dichloromethane;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1346243-42-2
C₂₇H₃₅N₇O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: caesium carbonate / 1,2-dimethoxyethane; water / 1 h / 60 °C

1.2: 0.5 h / 60 °C

2.1: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

3.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 72 h / 85 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

4.2: Cooling with ice

5.1: triethylamine / dichloromethane / 3 h / 5 - 20 °C / Inert atmosphere

6.1: acetonitrile / 18 h / 100 °C / sealed vessel

7.1: trifluoroacetic acid / dichloromethane / 18 h / 10 - 20 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; caesium carbonate; triethylamine; trifluoroacetic acid; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetonitrile;

Reference yield:

: 1083326-12-8
7-bromo-2-(1H-pyrazol-4-yl)quinoxaline

: 1346243-42-2
C₂₇H₃₅N₇O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 0 - 5 °C / Inert atmosphere

1.2: 18 h / 5 - 20 °C / Inert atmosphere

2.1: caesium carbonate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 72 h / 85 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.2: Cooling with ice

4.1: triethylamine / dichloromethane / 3 h / 5 - 20 °C / Inert atmosphere

5.1: acetonitrile / 18 h / 100 °C / sealed vessel

6.1: trifluoroacetic acid / dichloromethane / 18 h / 10 - 20 °C

With tetrabutyl ammonium fluoride; sodium hydride; caesium carbonate; triethylamine; trifluoroacetic acid; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;