2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan

Base Information

• Chemical Name: 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan
• CAS No.: 67437-13-2
• Molecular Formula: C₃₁H₂₆Cl₂
• Molecular Weight: 469.453

Synonyms:2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan

Chemical Property of 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan

Chemical Property:

Purity/Quality:

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Technology Process of 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan

There total 3 articles about 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromochlorobenzene (106-39-8) → 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan (67437-13-2)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) Mg, (ii) /BRN= 2133370/

2: POCl₃ / pyridine

3: 2-methyl-propan-2-ol / Irradiation

With trichlorophosphate; In pyridine; tert-butyl alcohol;

DOI:10.1021/ja00481a024

Reference yield:

1,1-Bis-(p-chlorphenyl)-3,3-dimethyl-5,5-diphenyl-4-penten-1-ol (67437-06-3) → 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan (67437-13-2)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃ / pyridine

2: 2-methyl-propan-2-ol / Irradiation

With trichlorophosphate; In pyridine; tert-butyl alcohol;

DOI:10.1021/ja00481a024

Reference yield:

1,1-bis(p-chlorophenyl)-3,3-dimethyl-5,5-diphenyl-1,4-pentadiene (54008-17-2) → 2,2-Dimethyl-1,1-diphenyl)-3-(2,2-bis-(p-chlorphenyl)-vinyl)-cyclopropan (67437-13-2)

Guidance literature:

In tert-butyl alcohol; Irradiation;

DOI:10.1021/ja00481a024

upstream raw materials:

1,1-bis(p-chlorophenyl)-3,3-dimethyl-5,5-diphenyl-1,4-pentadiene

bromochlorobenzene

1,1-Bis-(p-chlorphenyl)-3,3-dimethyl-5,5-diphenyl-4-penten-1-ol

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