1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

Base Information

Chemical Name:1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate
CAS No.:1596368-04-5
Molecular Formula:C₂₀H₂₁I₃N₂O₉
Molecular Weight:814.108
Hs Code.:

Synonyms:1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

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Chemical Property of 1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

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Technology Process of 1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

There total 4 articles about 1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 117-96-4
diatrizoic acid

: 143869-74-3
HEMA-1-chloroethyl carbonate

: 1596368-04-5
1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

Guidance literature:: diatrizoic acid; With caesium carbonate; In methanol; for 0.75h;

HEMA-1-chloroethyl carbonate; In N,N-dimethyl-formamide; at 100 ℃; Inert atmosphere;

Reference yield: 18.0%

: 143869-74-3
HEMA-1-chloroethyl carbonate

: C₁₁H₈I₃N₂O₄^(1-)*Cs⁽¹⁺⁾

: 1596368-04-5
1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

Guidance literature:: In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.25h; Inert atmosphere;

Reference yield:

: 868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5
2-methyl-2-propenoic acid 2-hydroxyethyl ester

: 1596368-04-5
1-((2-(2-methacryloyloxy)ethoxy)carbonyloxy)ethyl 3,5-diacetamido-2,4,6-triiodobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / diethyl ether / 0.5 h / 4 - 10 °C / Inert atmosphere

2: N,N-dimethyl-formamide / 1.25 h / 0 - 20 °C / Inert atmosphere

With pyridine; In diethyl ether; N,N-dimethyl-formamide;