4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

Base Information

Chemical Name:4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one
CAS No.:872050-98-1
Molecular Formula:C₂₂H₂₈O₇
Molecular Weight:404.46
Hs Code.:

Synonyms:4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

Suppliers and Price of 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

There total 12 articles about 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 944389-17-7
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-ol

: 872050-98-1
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

Guidance literature:: With 4-methyl-morpholine; tetrapropylammonium perruthennate; 4 A molecular sieve; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2007.02.033

Reference yield:

: 944389-16-6
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)but-3-yn-2-ol

: 872050-98-1
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / potassium bicarbonate; hydrogen / palladium on carbon / ethyl acetate / 20 °C

2: 98 percent / tetra-n-propylammonium perruthenate; 4-methylmorpholine; molecular sieves 4 Angstroem / CH₂Cl₂ / 20 °C

With 4-methyl-morpholine; tetrapropylammonium perruthennate; 4 A molecular sieve; hydrogen; potassium hydrogencarbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1016/j.tet.2007.02.033

Reference yield:

: 13391-35-0
allyl (4-methoxyphenyl) ether

: 872050-98-1
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(5-methoxy-2-(methoxymethoxy)phenyl)butan-2-one

Guidance literature:: Multi-step reaction with 6 steps

1.1: 84 percent / m-xylene / 180 °C

2.1: sodium hydride / dimethylformamide / 0.5 h / 0 °C

2.2: 80 percent / dimethylformamide / 1 h / 20 °C

3.1: 51 percent / osmium tetroxide; sodium periodate / tetrahydrofuran; H₂O / 8.5 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

4.2: 67 percent / tetrahydrofuran / -78 - 20 °C

5.1: 97 percent / potassium bicarbonate; hydrogen / palladium on carbon / ethyl acetate / 20 °C

6.1: 98 percent / tetra-n-propylammonium perruthenate; 4-methylmorpholine; molecular sieves 4 Angstroem / CH₂Cl₂ / 20 °C

With 4-methyl-morpholine; sodium periodate; osmium(VIII) oxide; n-butyllithium; tetrapropylammonium perruthennate; 4 A molecular sieve; hydrogen; sodium hydride; potassium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; m-xylene; 1.1: Claisen rearrangement;
DOI:10.1016/j.tet.2007.02.033