3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

Base Information

Chemical Name:3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane
CAS No.:1345882-03-2
Molecular Formula:C₁₄H₁₇BrF₂O₅
Molecular Weight:383.187
Hs Code.:

Synonyms:3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

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Technology Process of 3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

There total 6 articles about 3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1345881-95-9
3-(bromomethyl)-3-(methoxymethyl)oxetane

: 1345881-99-3
6-bromo-3-(difluoromethoxy)-2-methoxyphenol

: 1345882-03-2
3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

Guidance literature:: With potassium carbonate; In acetonitrile; at 80 ℃; for 16h;

Reference yield:

: 87-66-1
2-hydroxyresorcinol

: 1345882-03-2
3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

Guidance literature:: Multi-step reaction with 6 steps

1: potassium hydrogencarbonate / acetone / 16 h / Reflux

2: N-Bromosuccinimide / tetrahydrofuran / 2 h / -78 °C

3: potassium carbonate / acetone / 7 h / 0 - 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

5: hydrogenchloride; water / methanol / 1 h / 50 °C

6: potassium carbonate / acetonitrile / 16 h / 80 °C

With hydrogenchloride; N-Bromosuccinimide; water; potassium carbonate; potassium hydrogencarbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 29267-67-2
2-methoxyresorcinol

: 1345882-03-2
3-((6-bromo-3-(difluoromethoxy)-2-methoxyphenoxy)methyl)-3-(methoxymethyl)oxetane

Guidance literature:: Multi-step reaction with 5 steps

1: N-Bromosuccinimide / tetrahydrofuran / 2 h / -78 °C

2: potassium carbonate / acetone / 7 h / 0 - 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

4: hydrogenchloride; water / methanol / 1 h / 50 °C

5: potassium carbonate / acetonitrile / 16 h / 80 °C

With hydrogenchloride; N-Bromosuccinimide; water; potassium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone; acetonitrile;