2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

Base Information

Chemical Name:2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate
CAS No.:1161881-13-5
Molecular Formula:C₂₉H₃₁BrN₄O₉
Molecular Weight:659.491
Hs Code.:

Synonyms:2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

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Chemical Property of 2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

There total 1 articles about 2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1161880-94-9
2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride

: 39508-07-1
Ddz-L-Phe-OH

: 1161881-13-5
2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

: 67932-53-0
5,7-dinitroindoline

Guidance literature:: Ddz-L-Phe-OH; With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; at -20 ℃; for 1h; Inert atmosphere;

2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride; With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo900442p

Reference yield: 69.0%

: 1161881-13-5
2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

: 1161881-35-1
2-(3,5-dimethoxyphenyl)propan-2-yl (S)-1-(5,7-dinitroindolin-1-yl)-1-oxo-3-phenylpropan-2-ylcarbamate

Guidance literature:: With potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 2-(dicyclohexylphosphino)-2'-methylbiphenyl; In toluene; acetonitrile; at 100 ℃; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jo900442p