C₄₈H₆₃N₇O₉S

Base Information

Chemical Name:C₄₈H₆₃N₇O₉S
CAS No.:189563-94-8
Molecular Formula:C₄₈H₆₃N₇O₉S
Molecular Weight:914.136
Hs Code.:

C<sub>48</sub>H<sub>63</sub>N<sub>7</sub>O<sub>9</sub>S

Synonyms:C₄₈H₆₃N₇O₉S

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Chemical Property of C₄₈H₆₃N₇O₉S

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Technology Process of C₄₈H₆₃N₇O₉S

There total 4 articles about C₄₈H₆₃N₇O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 189563-90-4
C₂₇H₃₇N₅O₈S

: L-valyl-L-phenylalaninol benzyl ester p-toluenesulfonic acid salt

: 189563-94-8
C₄₈H₆₃N₇O₉S

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;
DOI:10.1246/cl.1997.345

Reference yield:

: 16874-17-2
L-phenylalanine tert-butyl ester

: 189563-94-8
C₄₈H₆₃N₇O₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 85.9 percent / acetonitrile / 2.5 h / 20 °C

2.1: N-methylmorpholine / CH₂Cl₂

2.2: 70 percent / CH₂Cl₂ / 24 h / 20 °C

3.1: 99 percent / H₂ / Pd/C / acetic acid / 2.5 h / 20 °C

4.1: N-methylmorpholine / tetrahydrofuran / 0 °C

4.2: 90 percent / EDCI; HOBt / CH₂Cl₂ / 0 - 20 °C

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/S0040-4020(01)00323-4

Reference yield:

: 189563-82-4
L-phenylalanine t-butyl ester N-hydroxysuccinimide carboxamide

: 189563-94-8
C₄₈H₆₃N₇O₉S

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-methylmorpholine / CH₂Cl₂

1.2: 70 percent / CH₂Cl₂ / 24 h / 20 °C

2.1: 99 percent / H₂ / Pd/C / acetic acid / 2.5 h / 20 °C

3.1: N-methylmorpholine / tetrahydrofuran / 0 °C

3.2: 90 percent / EDCI; HOBt / CH₂Cl₂ / 0 - 20 °C

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)00323-4