C₁₇H₁₈Cl₃NO₅

Base Information

Chemical Name:C₁₇H₁₈Cl₃NO₅
CAS No.:1123186-20-8
Molecular Formula:C₁₇H₁₈Cl₃NO₅
Molecular Weight:422.693
Hs Code.:

C<sub>17</sub>H<sub>18</sub>Cl<sub>3</sub>NO<sub>5</sub>

Synonyms:C₁₇H₁₈Cl₃NO₅

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Chemical Property of C₁₇H₁₈Cl₃NO₅

Chemical Property:

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Technology Process of C₁₇H₁₈Cl₃NO₅

There total 1 articles about C₁₇H₁₈Cl₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 4136-95-2
2,4,6-trichlorobenzoyl chloride

: 1123186-20-8
C₁₇H₁₈Cl₃NO₅

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol302309c

Reference yield:

: 1403235-24-4
C₂₀H₃₄O₂

: 1123186-20-8
C₁₇H₁₈Cl₃NO₅

: 1403235-37-9
C₃₀H₄₉NO₅

Guidance literature:: With dmap; In toluene; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol302309c

Reference yield:

: 1123186-20-8
C₁₇H₁₈Cl₃NO₅

: C₆₂H₈₅N₅O₁₁S

Guidance literature:: Multi-step reaction with 16 steps

1.1: dmap / toluene / 3 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol

3.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 2 h / 20 °C / Molecular sieve; Inert atmosphere

4.1: dicyclohexylboron chloride; N,N-dimethyl-ethanamine / diethyl ether; hexane / 1.5 h / 0 °C / Inert atmosphere

4.2: 26 h / -78 - -20 °C / Inert atmosphere

5.1: t-butyldimethylsiyl triflate / dichloromethane / 2 h / -50 °C / Inert atmosphere

6.1: potassium carbonate / methanol / 2 h / 20 °C / Inert atmosphere

6.2: 16 h / 20 °C / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0.08 h / Inert atmosphere

7.2: 20 °C / Inert atmosphere

8.1: 2,6-dimethylpyridine; t-butyldimethylsiyl triflate / dichloromethane / 1 h / 20 °C / Inert atmosphere

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane; tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

11.1: dmap; pyridine / dichloromethane / 1.08 h / 0 - 20 °C / Inert atmosphere

12.1: Triphenylphosphine oxide; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / 0 °C / Inert atmosphere

13.1: ammonium acetate; zinc / water; tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

14.1: N-methylaniline; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

15.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / Inert atmosphere

16.1: N-methylaniline; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; N,N-dimethyl-ethanamine; trifluoromethylsulfonic anhydride; palladium 10% on activated carbon; t-butyldimethylsiyl triflate; dicyclohexylboron chloride; ammonium acetate; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; HATU; N-methylaniline; Triphenylphosphine oxide; zinc; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; toluene;
DOI:10.1021/ol302309c