Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl

Base Information

Chemical Name:Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl
CAS No.:166267-91-0
Molecular Formula:C₅₅H₆₅N₇O₁₄S
Molecular Weight:1080.23
Hs Code.:

Synonyms:Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl

Chemical Property:

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Technology Process of Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl

There total 1 articles about Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 94604-79-2
pyroglutamic acid pentafluorophenyl ester

: (S)-2-{(R)-3-(Acetylamino-methylsulfanyl)-2-[(S)-2-((S)-2-amino-4-benzyloxycarbonyl-butyrylamino)-3-benzyloxycarbonyl-propionylamino]-propionylamino}-6-benzyloxycarbonylamino-hexanoic acid benzyl ester; compound with trifluoro-acetic acid

: 166267-91-0
Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 166267-91-0
Glp-Glu(OBzl)-Asp(OBzl)-Cys(Acm)-Lys(Z)-OBzl

: 84588-89-6
Glp-Glu-Asp-Cys-Lys-OH

Guidance literature:: Multi-step reaction with 3 steps

1: 49.6 percent / trifluoromethanesulfonic acid, trifluoroacetic acid, diethyl sulfide, m-cresol / 4 h / 0 °C

2: 75 percent / I₂, AcOH / 2 h / 20 °C

3: 58 percent / AcONa, triphenylphosphine, 80percent aq. AcOH / 170 h / 20 °C

With diethyl sulphide; trifluorormethanesulfonic acid; iodine; sodium acetate; acetic acid; 3-methyl-phenol; triphenylphosphine; trifluoroacetic acid;