3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Name:3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:1334630-52-2
Molecular Formula:C₅₄H₆₀N₂O₁₄Si
Molecular Weight:989.161
Hs Code.:

3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Synonyms:3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of 3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of 3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 3 articles about 3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1334630-47-5
3-(benzyloxycarbonylamino)propyl 6-O-t-butyldiphenylsilyl-2-deoxy-4-O-(2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-2-phthalimido-β-D-glucopyranoside

: 1334630-52-2
3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: 3-(benzyloxycarbonylamino)propyl 6-O-t-butyldiphenylsilyl-2-deoxy-4-O-(2,3-di-O-acetyl-4,6-O-benzylidene-β-D-galactopyranosyl)-2-phthalimido-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

In methanol; Inert atmosphere;
DOI:10.1016/j.carres.2011.07.002

Reference yield:

: 347391-77-9
3-benzyloxycarbonylamino-1-propyl 6-O-tert-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 1334630-52-2
3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 0.5 h / -40 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 0.5 h / 20 °C / Inert atmosphere

2.2: Amberlite-IR 120 (H+) / Inert atmosphere

With sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.carres.2011.07.002

Reference yield:

: 147332-52-3
ethyl 2,3-di-O-acetyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

: 1334630-52-2
3-(benzyloxycarbonylamino)propyl 4-O-(4,6-O-benzylidene-β-D-galactopyranosyl)-6-O-t-butyldiphenylsilyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 0.5 h / -40 °C / Inert atmosphere; Molecular sieve

2.1: sodium methylate / methanol / 0.5 h / 20 °C / Inert atmosphere

2.2: Amberlite-IR 120 (H+) / Inert atmosphere

With sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.carres.2011.07.002