7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester

Base Information

• Chemical Name: 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester
• CAS No.: 81424-28-4
• Molecular Formula: C₂₈H₄₀O₄
• Molecular Weight: 440.623

Synonyms:7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester

Chemical Property of 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester

Chemical Property:

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Technology Process of 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester

There total 6 articles about 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

7-[(1R,2S,3R)-2-((E)-(S)-3-Hydroxy-oct-1-enyl)-5-oxo-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester (78407-39-3) → 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester (81424-28-4)

Guidance literature:

With manganese(IV) oxide;

DOI:10.1021/jo00134a011

Reference yield:

prostaglandin A2 (13345-50-1) → 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester (81424-28-4)

Guidance literature:

Multi-step reaction with 6 steps

1: 100 percent / CH₂N₂ / diethyl ether

2: 78 percent

3: 73 percent / CuI

4: 100 percent / H₂

5: 54 percent

6: 85 percent / MnO₂

With diazomethane; manganese(IV) oxide; copper(l) iodide; hydrogen; In diethyl ether;

DOI:10.1021/jo00134a011

Reference yield:

(5Z,13E)-15-hydroxy-9-oxoprosta 5,10,13 trien-1-oic acid (31753-19-2) → 7-[(1R,2S,3R)-5-Oxo-2-((E)-3-oxo-oct-1-enyl)-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester (81424-28-4)

Guidance literature:

Multi-step reaction with 5 steps

1: 78 percent

2: 73 percent / CuI

3: 100 percent / H₂

4: 54 percent

5: 85 percent / MnO₂

With manganese(IV) oxide; copper(l) iodide; hydrogen;

DOI:10.1021/jo00134a011

upstream raw materials:

7-[(1R,2S,3R)-2-((E)-(S)-3-Hydroxy-oct-1-enyl)-5-oxo-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester

prostaglandin A₂

(5Z,13E)-15-hydroxy-9-oxoprosta 5,10,13 trien-1-oic acid

(Z)-7-{(1R,5S)-2-Oxo-5-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopent-3-enyl}-hept-5-enoic acid methyl ester

Downstream raw materials:

7-[(1R,2S,3R)-2-((E)-3-Hydroxy-oct-1-enyl)-5-oxo-3-phenyl-cyclopentyl]-heptanoic acid ethyl ester

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