(2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

Base Information

Chemical Name:(2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol
CAS No.:1384953-27-8
Molecular Formula:C₅₈H₉₇NO₈Si₂
Molecular Weight:992.581
Hs Code.:

Synonyms:(2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

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Technology Process of (2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

There total 1 articles about (2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1384953-26-7
C₇₃H₁₀₇NO₁₀Si₂

: 1384953-27-8
(2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 5h;
DOI:10.1016/j.bmc.2012.05.073

Reference yield: 93.0%

: 154027-13-1
n-tetracosyl isocyanate

: 1384953-27-8
(2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

: 1384953-35-8
(2S,3S,4R)-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)-2-(3-(n-tetracosyl)ureido)octadecane-1,3,4-triol

Guidance literature:: In chloroform; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.bmc.2012.05.073

Reference yield:

: 1384953-27-8
(2S,3S,4R)-2-amino-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-3,4-bis-O-(tert-butyldimethylsilyl)octadecane-1,3,4-triol

: 1384953-39-2
(2S,3S,4R)-1-O-(2,3,4-tri-O-benzyl-6-O-methyl-α-D-galactopyranosyl)-2-(3-(n-tetracosyl)ureido)octadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 16 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 17 h / 20 °C

With tetrabutyl ammonium fluoride; In tetrahydrofuran; chloroform;
DOI:10.1016/j.bmc.2012.05.073