C₃₃H₃₆O₈S₂

Base Information

Chemical Name:C₃₃H₃₆O₈S₂
CAS No.:1352274-37-3
Molecular Formula:C₃₃H₃₆O₈S₂
Molecular Weight:624.776
Hs Code.:

C<sub>33</sub>H<sub>36</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₃₃H₃₆O₈S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₆O₈S₂

Chemical Property:

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Technology Process of C₃₃H₃₆O₈S₂

There total 5 articles about C₃₃H₃₆O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1352274-36-2
C₁₉H₂₄O₄

: 98-59-9
p-toluenesulfonyl chloride

: 1352274-37-3
C₃₃H₃₆O₈S₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 24h; Cooling with ice;
DOI:10.1039/c1cc15219j

Reference yield:

: 20120-35-8
4-allylbiphenyl

: 1352274-37-3
C₃₃H₃₆O₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: osmium(VIII) oxide; potassium carbonate sesquihydrate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 20 h / 20 °C

1.2: 4 h

2.1: sodium hydride / 1,2-dimethoxyethane / 23 h / Inert atmosphere; Reflux

3.1: ozone / methanol / 0.92 h

3.2: 1 h / Inert atmosphere

3.3: 2 h

4.1: dmap; triethylamine / dichloromethane / 24 h / 20 °C / Cooling with ice

With dmap; osmium(VIII) oxide; potassium carbonate sesquihydrate; sodium hydride; ozone; triethylamine; potassium hexacyanoferrate(III); In methanol; 1,2-dimethoxyethane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c1cc15219j

Reference yield:

: 30991-11-8
3-(biphenyl-4-yl)propane-1,2-diol

: 1352274-37-3
C₃₃H₃₆O₈S₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / 1,2-dimethoxyethane / 23 h / Inert atmosphere; Reflux

2.1: ozone / methanol / 0.92 h

2.2: 1 h / Inert atmosphere

2.3: 2 h

3.1: dmap; triethylamine / dichloromethane / 24 h / 20 °C / Cooling with ice

With dmap; sodium hydride; ozone; triethylamine; In methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1039/c1cc15219j