(2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

Base Information

Chemical Name:(2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine
CAS No.:171019-31-1
Molecular Formula:C₁₅H₂₁NOS
Molecular Weight:263.404
Hs Code.:

Synonyms:(2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

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Chemical Property of (2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

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Technology Process of (2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

There total 4 articles about (2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 171019-27-5
(2S,3S,3aS)-2-Methyl-3-((R)-toluene-4-sulfinyl)-hexahydro-isoxazolo[2,3-a]pyridine

: 171019-31-1
(2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

Guidance literature:: With trimethylsilyl iodide; sodium iodide; In acetonitrile; Ambient temperature;
DOI:10.1016/S0957-4166(96)00480-6

Reference yield:

: 34418-91-2
2,3,4,5-tetrahydropyridine N-oxide

: 171019-31-1
(2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / diethyl ether / Ambient temperature

2: 90 percent / Me₃SiI, NaI / acetonitrile / Ambient temperature

With trimethylsilyl iodide; sodium iodide; In diethyl ether; acetonitrile;
DOI:10.1016/S0957-4166(96)00480-6

Reference yield:

: 4801-58-5
N-hydroxypiperidine

: 171019-31-1
(2S,3S,3aS)-2-Methyl-3-p-tolylsulfanyl-hexahydro-isoxazolo[2,3-a]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: HgO / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 89 percent / diethyl ether / Ambient temperature

3: 90 percent / Me₃SiI, NaI / acetonitrile / Ambient temperature

With trimethylsilyl iodide; sodium iodide; mercury(II) oxide; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/S0957-4166(96)00480-6