C₃₉H₆₃NO₆SSi

Base Information

• Chemical Name: C₃₉H₆₃NO₆SSi
• CAS No.: 1262283-53-3
• Molecular Formula: C₃₉H₆₃NO₆SSi
• Molecular Weight: 702.084
• Mol file: 1262283-53-3.mol

Synonyms:C₃₉H₆₃NO₆SSi

Chemical Property of C₃₉H₆₃NO₆SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₉H₆₃NO₆SSi

There total 4 articles about C₃₉H₆₃NO₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(tert-butyloxycarbonyl)amino]octadecan-3,4-diol (1224436-76-3) → C39H63NO6SSi (1262283-53-3)

Guidance literature:

With thionyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/jo101757k

Reference yield:

D-ribo-phytosphingosine (554-62-1) → C39H63NO6SSi (1262283-53-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; water / 0 - 20 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/jo101757k

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → C39H63NO6SSi (1262283-53-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; water / 0 - 20 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With dmap; thionyl chloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1021/jo101757k

upstream raw materials:

(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(tert-butyloxycarbonyl)amino]octadecan-3,4-diol

D-ribo-phytosphingosine

di-tert-butyl dicarbonate

tert-butyl [(2S,3S,4R)-1,3,4-trihydroxyoctadecan-2-yl]carbamate

Downstream raw materials:

(2S,3S,4R)-1-(tert-butyldiphenylsilyloxy)-2-[N-(tert-butyloxycarbonyl)amino]octadecan-3,4-cyclic sulfate

(4S,5R)-4-((tert-butyldiphenylsilyloxy)methyl)-5-((R)-1-hydroxypentadecyl)oxazolidin-2-one

(4S,5S,6S)-4-((tert-butyldiphenylsilyloxy)methyl)-5-hydroxy-6-tetradecyl-1,3-oxazinan-2-one