3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

Base Information

Chemical Name:3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide
CAS No.:1070892-63-5
Molecular Formula:C₂₄H₃₁BrClN₅O₃Si
Molecular Weight:580.984
Hs Code.:

Synonyms:3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

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Chemical Property of 3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

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Technology Process of 3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

There total 7 articles about 3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1070892-62-4
3-bromo-4-chloro-N-methyl-N-{2-[3-(1H-tetrazol-5-yl)-propoxy]-phenyl}-benzamide

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1070892-63-5
3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

: 1070893-16-1
3-bromo-4-chloro-N-methyl-N-(2-{3-[2-(2-trimethylsilanyl-ethoxymethyl)-2H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

: 42860-10-6
3-bromo-4-chlorobenzoic acid

: 1070892-63-5
3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

: 1070893-16-1
3-bromo-4-chloro-N-methyl-N-(2-{3-[2-(2-trimethylsilanyl-ethoxymethyl)-2H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h

2.1: sodium hydrogencarbonate / water; acetonitrile / 1.5 h

2.2: 16 h / 20 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

4.1: triethylaluminum; azido tributyltin (IV) / toluene / 5 h / 80 °C

4.2: 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

With oxalyl dichloride; triethylaluminum; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; azido tributyltin (IV); N,N-dimethyl-formamide; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 21900-34-5
3-bromo-4-chlorobenzoyl chloride

: 1070892-63-5
3-bromo-4-chloro-N-methyl-N-(2-{3-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

: 1070893-16-1
3-bromo-4-chloro-N-methyl-N-(2-{3-[2-(2-trimethylsilanyl-ethoxymethyl)-2H-tetrazol-5-yl]-propoxy}-phenyl)-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / water; acetonitrile / 1.5 h

1.2: 16 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

3.1: triethylaluminum; azido tributyltin (IV) / toluene / 5 h / 80 °C

3.2: 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

With triethylaluminum; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; azido tributyltin (IV); In water; N,N-dimethyl-formamide; toluene; acetonitrile;