C₃₈H₆₀O₁₀

Base Information

• Chemical Name: C₃₈H₆₀O₁₀
• CAS No.: 929296-60-6
• Molecular Formula: C₃₈H₆₀O₁₀
• Molecular Weight: 676.888
• Mol file: 929296-60-6.mol

Synonyms:C₃₈H₆₀O₁₀

Chemical Property of C₃₈H₆₀O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₆₀O₁₀

There total 37 articles about C₃₈H₆₀O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.3%

1-(methoxycarbonyl)pentadec-10(S)-yl 4-O-benzyl-α-L-rhamnopyranosyl-(1→4)-2,3-O-isopropylidene-α-L-rhamnopyranoside (1513847-22-7) → C38H60O10 (929296-60-6) + C38H60O10

Guidance literature:

With triphenylphosphine; In toluene; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ol403369h

Reference yield:

C38H60O10 → C38H60O10 (929296-60-6)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In toluene; at 0 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol403369h

Reference yield:

(S)-methyl 11-hydroxyhexadecanoate (121043-05-8) → C38H60O10 (929296-60-6)

Guidance literature:

Multi-step reaction with 7 steps

1: 66 percent / boron trifluoride-diethyl ether / CH₂Cl₂ / -78 - 20 °C

2: NaOMe / methanol / -20 °C

3: p-TsOH / dimethylformamide / 20 °C

4: 96 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / -78 - 20 °C

5: 94 percent / potassium hydroxide / methanol; H₂O / 55 °C

6: triphenylphosphine / toluene / 6 h / 20 °C

7: 58 percent / toluene / 168 h / Heating

With potassium hydroxide; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; triphenylphosphine; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

DOI:10.1055/s-2006-956493

upstream raw materials:

acetic acid 11-hydroxy-1-pentyl-undecyl ester

(S)-1-benzyloxy-11-hexadecanol

acetic acid 11-benzyloxy-1-pentyl-undecyl ester

1-(hydroxycarbonyl)pentadec-10(S)-yl 4-O-benzyl-α-L-rhamnopyranosyl-(1→4)-2,3-O-isopropylidene-α-L-rhamnopyranoside