phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane

Base Information

Chemical Name:phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane
CAS No.:121920-80-7
Molecular Formula:CH₂Cl₂*C₃₄H₃₇P₃S₃
Molecular Weight:719.72
Hs Code.:

Synonyms:phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane

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Chemical Property of phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane

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Technology Process of phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane

There total 1 articles about phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 10544-50-0
sulfur

: 121935-47-5
bromo{phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine}nickel(II) bromide-dichloromethane

: 121920-80-7
phenylbis(5,6-dimethyl-7-phenyl-7-phosphabicyclo{2.2.1}hept-5-en-2-yl)phosphine P,P',P''-trisulfide * dichloromethane

Guidance literature:: With NaCN; In dichloromethane; water; Under N2, addn. of a satd. aq. NaCN soln. to a soln. of Ni-complex in CH2Cl2, agitating with N2-stream for 45 min, sepg. of CH2Cl2 layer, filtn., addn. of S8 and 1-methylimidazole, stirring (room temp., 12 h, N2).; Concg., addn. of hexane, standing overnight, filtn., recrystn. (CH2Cl2/hexane), vac. drying, elem. anal.;
DOI:10.1021/ic00317a012