methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate

Base Information

• Chemical Name: methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate
• CAS No.: 1456601-82-3
• Molecular Formula: C₃₀H₂₇ClN₂O₆S
• Molecular Weight: 579.073

Synonyms:methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate

Chemical Property of methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate

Chemical Property:

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Technology Process of methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate

There total 5 articles about methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

methyl 5-(4-chlorobenzylamino)-2-hydroxybenzoate (1456601-59-4) + 2-(N-methylbiphenyl-4-ylsulfonamido)acetic acid (381193-32-4) → methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate (1456601-82-3)

Guidance literature:

With dichlorotriphenylphosphorane; In dichloromethane; at 80 ℃; for 1h; Inert atmosphere; Microwave irradiation;

DOI:10.1039/c3md20323a

Reference yield:

4-chlorobenzaldehyde (104-88-1) → methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate (1456601-82-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / methanol / 1 h / 20 - 40 °C / Molecular sieve

1.2: 2 h / 5 - 20 °C

2.1: dichlorotriphenylphosphorane / dichloromethane / 1 h / 80 °C / Inert atmosphere; Microwave irradiation

With acetic acid; dichlorotriphenylphosphorane; In methanol; dichloromethane;

DOI:10.1039/c3md20323a

Reference yield:

methyl 5-amino-2-hydroxybenzoate (42753-75-3) → methyl 5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoate (1456601-82-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / methanol / 1 h / 20 - 40 °C / Molecular sieve

1.2: 2 h / 5 - 20 °C

2.1: dichlorotriphenylphosphorane / dichloromethane / 1 h / 80 °C / Inert atmosphere; Microwave irradiation

With acetic acid; dichlorotriphenylphosphorane; In methanol; dichloromethane;

DOI:10.1039/c3md20323a

upstream raw materials:

4-chlorobenzaldehyde

methyl 5-(4-chlorobenzylamino)-2-hydroxybenzoate

2-(N-methylbiphenyl-4-ylsulfonamido)acetic acid

methyl 5-amino-2-hydroxybenzoate

Downstream raw materials:

5-(N-(4-chlorobenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

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