3,3-dichloro-1,2-diphenylcyclopropene

Base Information

Chemical Name:3,3-dichloro-1,2-diphenylcyclopropene
CAS No.:2570-00-5
Molecular Formula:C₁₅H₁₀Cl₂
Molecular Weight:261.15
Hs Code.:

Synonyms:3,3-dichloro-1,2-diphenylcyclopropene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,3-dichloro-1,2-diphenylcyclopropene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 3,3-dichloro-1,2-diphenylcyclopropene

There total 7 articles about 3,3-dichloro-1,2-diphenylcyclopropene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 886-38-4
diphenylcyclopropenone

: 2570-00-5
3,3-dichloro-1,2-diphenylcyclopropene

Guidance literature:: With thionyl chloride; at 40 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c1dt10109a

Reference yield: 87.0%

: 52730-95-7
2,3-diphenylcyclopropenone

: 2570-00-5
3,3-dichloro-1,2-diphenylcyclopropene

Guidance literature:: With thionyl chloride; at 50 ℃; for 2h; Inert atmosphere; Neat (no solvent);
DOI:10.1021/ol102980t

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 2570-00-5
3,3-dichloro-1,2-diphenylcyclopropene

Guidance literature:: Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere; Sealed tube

1.2: Inert atmosphere; Sealed tube

2.1: thionyl chloride / dichloromethane / 2 h / 50 °C / Inert atmosphere; Sealed tube

With aluminum (III) chloride; thionyl chloride; In dichloromethane;
DOI:10.1021/acs.orglett.9b04656