Technology Process of C23H37NO4Si
There total 1 articles about C23H37NO4Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-(tert-butyldimethylsilyloxy)propyl bromide;
With
magnesium;
In
tetrahydrofuran;
(S)-1-allyl-3-(benzyloxy)pyrrolidine-2,5-dione;
In
tetrahydrofuran; dichloromethane;
at 0 ℃;
for 8h;
DOI:10.1039/c0cc04371k
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -55 - 20 °C
2.1: rhodium(III) trichloride hydrate / ethanol / 6 h / Reflux
2.2: 48 h / Reflux
2.3: 24 h / 0 - 20 °C / Reflux; Inert atmosphere
3.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere
4.1: dmap; triethylamine / dichloromethane / 24 h / 0 °C / Inert atmosphere
With
1H-imidazole; triethylsilane; dmap; rhodium(III) trichloride hydrate; boron trifluoride diethyl etherate; triethylamine;
In
ethanol; dichloromethane;
DOI:10.1039/c0cc04371k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / -55 - 20 °C
2.1: rhodium(III) trichloride hydrate / ethanol / 6 h / Reflux
2.2: 48 h / Reflux
2.3: 24 h / 0 - 20 °C / Reflux; Inert atmosphere
3.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere
With
1H-imidazole; triethylsilane; dmap; rhodium(III) trichloride hydrate; boron trifluoride diethyl etherate;
In
ethanol; dichloromethane;
DOI:10.1039/c0cc04371k
