allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

Base Information

Chemical Name:allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside
CAS No.:1573119-91-1
Molecular Formula:C₃₇H₆₂O₁₁Si₂
Molecular Weight:739.064
Hs Code.:

allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

Synonyms:allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

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Chemical Property of allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

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Technology Process of allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

There total 3 articles about allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1573119-87-5
allyl 2-O-acetyl-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

: 1573119-90-0
allyl 4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

: 1573119-91-1
allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3ra47523a

Reference yield:

: 1573119-89-7
C₂₃H₃₂Cl₃NO₇Si

: 1573119-90-0
allyl 4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

: 1573119-91-1
allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

1.2: 1.5 h / -15 °C / Inert atmosphere

2.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

With sodium methylate; In methanol; dichloromethane;
DOI:10.1039/c3ra47523a

Reference yield:

: C₂₁H₃₁BrO₆Si

: 1573119-90-0
allyl 4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

: 1573119-91-1
allyl 4,6-O-benzylidene-2-O-tert-butyldimethylsilyl-β-D-glucopyranosyl-(1→2)-6-O-tert-butyldimethylsilyl-3,4-O-isopropylidene-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.2: 1.5 h / -15 °C / Inert atmosphere

3.1: sodium methylate / methanol / 2 h / 20 °C / Inert atmosphere

With sodium methylate; potassium carbonate; In methanol; dichloromethane;
DOI:10.1039/c3ra47523a