4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

Base Information

Chemical Name:4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline
CAS No.:1402638-67-8
Molecular Formula:C₂₄H₂₃N₅
Molecular Weight:381.48
Hs Code.:

Synonyms:4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

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Chemical Property of 4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

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Technology Process of 4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

There total 5 articles about 4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1402638-66-7
6-(tris(4-nitrophenyl)methyl)pyridin-3-amine

: 1402638-67-8
4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1246/cl.2012.828

Reference yield:

: 1402638-63-4
6-tritylpyridine-3-amine

: 1402638-67-8
4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1 h / 20 °C

2: nitric acid; acetic anhydride; acetic acid / 0 °C

3: methanol; water; potassium hydroxide / tetrahydrofuran / 25 h / Reflux

4: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 4 h / 20 °C

With pyridine; methanol; palladium 10% on activated carbon; water; hydrogen; nitric acid; acetic anhydride; acetic acid; potassium hydroxide; In tetrahydrofuran;
DOI:10.1246/cl.2012.828

Reference yield:

: 1402638-64-5
N-(6-tritylpyridin-3-yl)acetamid

: 1402638-67-8
4,4',4''-((5-aminopyridin-2-yl)methanetriyl)trianiline

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; acetic anhydride; acetic acid / 0 °C

2: methanol; water; potassium hydroxide / tetrahydrofuran / 25 h / Reflux

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 4 h / 20 °C

With methanol; palladium 10% on activated carbon; water; hydrogen; nitric acid; acetic anhydride; acetic acid; potassium hydroxide; In tetrahydrofuran;
DOI:10.1246/cl.2012.828