C₃₇H₅₄N₆O₁₀

Base Information

Chemical Name:C₃₇H₅₄N₆O₁₀
CAS No.:1579275-65-2
Molecular Formula:C₃₇H₅₄N₆O₁₀
Molecular Weight:742.87
Hs Code.:

C<sub>37</sub>H<sub>54</sub>N<sub>6</sub>O<sub>10</sub>

Synonyms:C₃₇H₅₄N₆O₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₅₄N₆O₁₀

Chemical Property:

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Technology Process of C₃₇H₅₄N₆O₁₀

There total 9 articles about C₃₇H₅₄N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₅₈N₆O₁₁S

: 1579275-65-2
C₃₇H₅₄N₆O₁₀

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In 2,2,2-trifluoroethanol; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo500039d

Reference yield:

: 1515605-52-3
C₁₄H₂₉N₃O₂Si

: 1579275-65-2
C₃₇H₅₄N₆O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: triethylphosphine / tetrahydrofuran; toluene / 30 h / 20 °C / Inert atmosphere

2: toluene / 48 h / 70 °C / Inert atmosphere

3: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere

4: triethylamine; dmap / acetonitrile / Inert atmosphere

5: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / 2,2,2-trifluoroethanol / 1 h / -78 °C / Inert atmosphere

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine tris(hydrogen fluoride); triethylamine; triethylphosphine; In tetrahydrofuran; 2,2,2-trifluoroethanol; toluene; acetonitrile; 1: |Staudinger Azide Reduction / 2: |Ugi Condensation;
DOI:10.1021/jo500039d

Reference yield:

: 1579275-63-0
(2R,3R)-tert-butyl 2-benzyloxycarbonylamino-3-tert-butoxycarbonylaminobutanoate

: 1579275-65-2
C₃₇H₅₄N₆O₁₀

Guidance literature:: Multi-step reaction with 6 steps

1: trifluoroacetic acid / dichloromethane / 12 h / 0 °C / Inert atmosphere

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

3: toluene / 48 h / 70 °C / Inert atmosphere

4: triethylamine tris(hydrogen fluoride) / acetonitrile / 24 h / 50 °C / Inert atmosphere

5: triethylamine; dmap / acetonitrile / Inert atmosphere

6: tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) / 2,2,2-trifluoroethanol / 1 h / -78 °C / Inert atmosphere

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydrogencarbonate; triethylamine tris(hydrogen fluoride); triethylamine; trifluoroacetic acid; In dichloromethane; 2,2,2-trifluoroethanol; N,N-dimethyl-formamide; toluene; acetonitrile; 3: |Ugi Condensation;
DOI:10.1021/jo500039d