2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide

Base Information

• Chemical Name: 2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide
• CAS No.: 93969-03-0
• Molecular Formula: C₁₉H₂₇N₃O₂
• Molecular Weight: 329.442

Synonyms:2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide

Chemical Property of 2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide

There total 1 articles about 2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Glycine xylidide (18865-38-8) + 3,5-Dibromo-4-oxo-2,2,6,6-tetramethylpiperidine Hydrobromide (19971-12-1) → 2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide (93969-03-0)

Guidance literature:

With potassium carbonate; In methanol; water; at 25 ℃; for 3h;

DOI:10.1021/jm00157a005

Reference yield: 50.0%

2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide (93969-03-0) → C19H26N3O3 (102132-43-4)

Guidance literature:

With 2Na⁽¹⁺⁾*2ClH*O₄W^(2-); dihydrogen peroxide; edetate disodium; In methanol; at 20 ℃; for 72h;

DOI:10.1021/jm00157a005

Reference yield:

2-(2,2,5,5-tetramethyl-2,5-dihydro-3-pyrroline-3-carbonylamino)-N-(2,6-dimethyl-phenyl)-acetamide (93969-03-0) → 2,2,5,5-Tetramethyl-pyrrolidine-3-carboxylic acid [(2,6-dimethyl-phenylcarbamoyl)-methyl]-amide (102132-29-6)

Guidance literature:

With hydrogen; palladium on activated charcoal; In chloroform; at 25 ℃; under 760 Torr;

DOI:10.1021/jm00157a005

upstream raw materials:

Glycine xylidide

3,5-Dibromo-4-oxo-2,2,6,6-tetramethylpiperidine Hydrobromide

Downstream raw materials:

C₁₉H₂₆N₃O₃

2,2,5,5-Tetramethyl-pyrrolidine-3-carboxylic acid [(2,6-dimethyl-phenylcarbamoyl)-methyl]-amide

C₁₉H₂₈N₃O₃

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