(R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

Base Information

Chemical Name:(R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol
CAS No.:1026392-30-2
Molecular Formula:C₂₈H₃₂O₃S
Molecular Weight:448.626
Hs Code.:

Synonyms:(R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

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Technology Process of (R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

There total 6 articles about (R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1027924-48-6
Thioacetic acid S-{(R)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-1-[((Z)-pent-2-enyl)oxymethyl]-ethyl} ester

: 1026392-30-2
(R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 55 ℃; for 1h;
DOI:10.1021/jm00050a009

Reference yield:

: 7348-78-9
(Z)-1-bromo-2-pentene

: 1026392-30-2
(R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaH / 1.) DMF, 45 min, 2.) DMF, 25 deg C, 14 h

2: 1 N HCl / methanol / 24 h / 25 °C

3: pyridine / tetrahydrofuran / 14 h / 25 °C

4: pyridine / CH₂Cl₂ / 14 h / 25 °C

5: dimethylformamide / 16 h / 80 °C

6: NaBH₄ / ethanol / 1 h / 55 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium hydride; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009

Reference yield:

: (R)-3-[((Z)-Pent-2-enyl)oxy]-propane-1,2-diol

: 1026392-30-2
(R)-1-[(4-Methoxy-phenyl)-diphenyl-methoxy]-3-[((Z)-pent-2-enyl)oxy]-propane-2-thiol

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / tetrahydrofuran / 14 h / 25 °C

2: pyridine / CH₂Cl₂ / 14 h / 25 °C

3: dimethylformamide / 16 h / 80 °C

4: NaBH₄ / ethanol / 1 h / 55 °C

With pyridine; sodium tetrahydroborate; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009