N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

Base Information

Chemical Name:N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide
CAS No.:1615654-17-5
Molecular Formula:C₂₆H₃₇NO₃
Molecular Weight:411.585
Hs Code.:

Synonyms:N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

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Chemical Property of N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

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Technology Process of N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

There total 6 articles about N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 2936-08-5
valproyl chloride

: 1615654-10-8
2-[4-[3-(methylamino)-1-phenylpropoxy]phenyl]ethanol

: 1615654-17-5
N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 48h;

Reference yield: 60.0%

: valproyl chloride

: 1615654-10-8
2-[4-[3-(methylamino)-1-phenylpropoxy]phenyl]ethanol

: 1615654-17-5
N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

Guidance literature:: With triethylamine; In hexane; ethyl acetate;

Reference yield:

: 42142-52-9
3-methylamino-1-phenylpropan-1-ol

: 1615654-17-5
N-[3-[4-(2-hydroxyethyl)phenoxy]-3-phenylpropyl]-N-methyl-2-propylpentanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / tetrahydrofuran / 20 h / 20 °C

2.1: triphenylphosphine; diethylazodicarboxylate / toluene / 21 h / 80 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.75 h / 0 - 20 °C / Inert atmosphere

3.2: 0.33 h / 0 °C

4.1: trifluoroacetic acid / dichloromethane / 0.75 h / 0 - 20 °C

5.1: triethylamine / dichloromethane / 48 h / 0 - 20 °C

With lithium aluminium tetrahydride; triethylamine; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene;