C₆₈H₁₁₂

Base Information

• Chemical Name: C₆₈H₁₁₂
• CAS No.: 325144-96-5
• Molecular Formula: C₆₈H₁₁₂
• Molecular Weight: 929.637
• Mol file: 325144-96-5.mol

Synonyms:C₆₈H₁₁₂

Chemical Property of C₆₈H₁₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₈H₁₁₂

There total 6 articles about C₆₈H₁₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-dibromo-1,4-di-N-dodecylbenzene (117635-23-1) → C68H112 (325144-96-5)

Guidance literature:

Multi-step reaction with 3 steps

1: BuLi / diethyl ether / 0 °C

2: amine / Pd/Cu

3: NaH / 1,2-dimethoxy-ethane / Heating

With n-butyllithium; sodium hydride; Pd/Cu; In 1,2-dimethoxyethane; diethyl ether; 3: Horner reaction;

DOI:10.1021/ja0010251

Reference yield:

4-bromo-2,5-didodecyl-benzaldehyde (325144-77-2) → C68H112 (325144-96-5)

Guidance literature:

Multi-step reaction with 2 steps

1: amine / Pd/Cu

2: NaH / 1,2-dimethoxy-ethane / Heating

With sodium hydride; Pd/Cu; In 1,2-dimethoxyethane; 2: Horner reaction;

DOI:10.1021/ja0010251

Reference yield:

2,5-didodecyl-4-prop-1-ynyl-benzaldehyde (325144-80-7) → C68H112 (325144-96-5)

Guidance literature:

Multi-step reaction with 4 steps

1: LiAlH₄ / tetrahydrofuran

2: DMAP / tetrahydrofuran

3: NaI

4: NaH / 1,2-dimethoxy-ethane / Heating

With dmap; lithium aluminium tetrahydride; sodium hydride; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; 3: Arbuzov reaction / 4: Horner reaction;

DOI:10.1021/ja0010251

upstream raw materials:

2,5-didodecyl-4-prop-1-ynyl-benzaldehyde

(2,5-didodecyl-4-prop-1-ynyl-benzyl)-phosphonic acid diethyl ester

2,5-dibromo-1,4-di-N-dodecylbenzene

4-bromo-2,5-didodecyl-benzaldehyde

Refernces