Technology Process of C62H77O20P3
There total 5 articles about C62H77O20P3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
benzyl 4-formyl-2-(octyloxy)phenyl diisopropylphosphoramidite; 1D-2,3,6-O-tris(methoxymethylene)-myo-inositol 4,5-bis(dibenzyl phosphate);
With
1H-tetrazole;
In
dichloromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
With
tert.-butylhydroperoxide;
In
decane; dichloromethane;
at -40 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C
2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate
3.1: 1H-tetrazole / dichloromethane / 3 h / 20 °C / Inert atmosphere
4.1: 1H-tetrazole / dichloromethane / 12 h / 20 °C / Inert atmosphere
4.2: -40 - 20 °C
With
1H-tetrazole; hydrogen; sodium hydride;
palladium 10% on activated carbon;
In
dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate
2.1: 1H-tetrazole / dichloromethane / 3 h / 20 °C / Inert atmosphere
3.1: 1H-tetrazole / dichloromethane / 12 h / 20 °C / Inert atmosphere
3.2: -40 - 20 °C
With
1H-tetrazole; hydrogen;
palladium 10% on activated carbon;
In
dichloromethane; ethyl acetate;