2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

Base Information

Chemical Name:2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate
CAS No.:914398-73-5
Molecular Formula:C₂₃H₃₄N₂O₈
Molecular Weight:466.532
Hs Code.:

Synonyms:2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

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Chemical Property of 2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

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Technology Process of 2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

There total 5 articles about 2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 914398-72-4
2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethanol

: 14661-69-9
(E)-2-(2-benzenesulfonylhydrazide)acetic acid chloride

: 914398-73-5
2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

Guidance literature:: 2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethanol; (E)-2-(2-benzenesulfonylhydrazide)acetic acid chloride; With N,N-dimethyl-aniline; In dichloromethane; at 0 ℃; for 1h;

With triethylamine; In dichloromethane; for 1h;
DOI:10.1021/jo0614902

Reference yield:

: 153901-22-5
methanesulfonic acid 2-propenyloxyethyl ester

: 914398-73-5
2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 61 percent / sodium hydride / tetrahydrofuran / 12 h / Heating

2.1: 74 percent / triethylamine / tetrahydrofuran / 1 h / 20 °C

3.1: 4.47 g / sodium hydride / tetrahydrofuran / 12 h / Heating

4.1: N,N-dimethylaniline / CH₂Cl₂ / 1 h / 0 °C

4.2: 76 percent / triethylamine / CH₂Cl₂ / 1 h

With sodium hydride; N,N-dimethyl-aniline; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0614902

Reference yield:

: 87048-14-4,27274-31-3
2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethan-1-ol

: 914398-73-5
2-(2-(2-(2-(2-(2-allyloxyethoxy)ethoxy)ethoxy)ethoxy)ethoxymethyl)phenylmethyl diazoacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 74 percent / triethylamine / tetrahydrofuran / 1 h / 20 °C

2.1: 4.47 g / sodium hydride / tetrahydrofuran / 12 h / Heating

3.1: N,N-dimethylaniline / CH₂Cl₂ / 1 h / 0 °C

3.2: 76 percent / triethylamine / CH₂Cl₂ / 1 h

With sodium hydride; N,N-dimethyl-aniline; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0614902