(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

Base Information

Chemical Name:(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene
CAS No.:160429-75-4
Molecular Formula:C₃₃H₅₂O₇
Molecular Weight:560.772
Hs Code.:

(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

Synonyms:(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

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Chemical Property of (2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

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Technology Process of (2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

There total 12 articles about (2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147033-10-1
(2R,3S)-2-ethyl-3-<<(2R,4S,3S,5S,6R)-2-(4-methoxyphenyl)-5-methyl-4-<(1R,2E)-1-methyl-2-butenyl>>-1,3-dioxan-6-yl>-3-methyl-1,4-dioxaspiro<4.4>nonane

: 160429-75-4
(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) O₃/O₂; 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C; 2.) CH₂Cl₂, -78 deg C to 0 deg C

2: 91 percent / CH₂Cl₂ / 24 h / Ambient temperature

3: 99 percent / LiAlH₄ / diethyl ether / 6 h / Heating

5: 1.) 0.35M iPrMgBr; 2.) LiAlH₄ / 1.) THF, 30 min; 2.) THF, reflux, 6 h

With lithium aluminium tetrahydride; isopropylmagnesium bromide; oxygen; ozone; triphenylphosphine; In diethyl ether; dichloromethane;

Reference yield:

: 147033-11-2
(2E,4R)-4-<(2R,4S,5S,6R)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-2-methyl-2-penten-1-ol

: 160429-75-4
(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) 0.35M iPrMgBr; 2.) LiAlH₄ / 1.) THF, 30 min; 2.) THF, reflux, 6 h

With lithium aluminium tetrahydride; isopropylmagnesium bromide;

Reference yield:

: 160625-13-8
(2S)-2-<(2R,4R,5S,6R)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-2-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>propanal

: 160429-75-4
(2E,4R,5R,6R,8R)-8-<(2R,4R,5S,6S)-6-<(2R,3S)-2-ethyl-3-methyl-1,4-dioxaspiro<4.4>nonan-3-yl>-4-<2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl>>-5,6-dihydroxy-4,6-dimethyl-2-nonene

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / CH₂Cl₂ / 24 h / Ambient temperature

2: 99 percent / LiAlH₄ / diethyl ether / 6 h / Heating

4: 1.) 0.35M iPrMgBr; 2.) LiAlH₄ / 1.) THF, 30 min; 2.) THF, reflux, 6 h

With lithium aluminium tetrahydride; isopropylmagnesium bromide; In diethyl ether; dichloromethane;