2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole

Base Information

• Chemical Name: 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole
• CAS No.: 110963-72-9
• Molecular Formula: C₂₂H₂₈N₄O
• Molecular Weight: 364.491

Synonyms:2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole

Chemical Property of 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole

There total 3 articles about 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

2-<(Hexahydro-4-methyl-1H-1,4-diazepin-1-yl)methyl>-1H-benzimidazole (95893-91-7) → 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole (110963-72-9)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

DOI:10.1002/jhet.5570240107

Reference yield:

1-Methylhomopiperazine (4318-37-0) → 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole (110963-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / ethanol; dimethylformamide / 2 h / 60 °C

2: 62 percent / sodium hydride / dimethylformamide / 2 h / 60 °C

With sodium hydride; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570240107

Reference yield:

2-chloromethyl-1H-benzimidazole (4857-04-9) → 2-(4-Methyl-[1,4]diazepan-1-ylmethyl)-1-(2-phenoxy-ethyl)-1H-benzoimidazole (110963-72-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 26 percent / ethanol; dimethylformamide / 2 h / 60 °C

2: 62 percent / sodium hydride / dimethylformamide / 2 h / 60 °C

With sodium hydride; In ethanol; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570240107

upstream raw materials:

2-<(Hexahydro-4-methyl-1H-1,4-diazepin-1-yl)methyl>-1H-benzimidazole

1-Methylhomopiperazine

2-chloromethyl-1H-benzimidazole

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