syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione

Base Information

• Chemical Name: syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione
• CAS No.: 164321-96-4
• Molecular Formula: C₁₆H₁₉N₃O₂
• Molecular Weight: 285.346

Synonyms:syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione

Chemical Property of syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione

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Technology Process of syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione

There total 4 articles about syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-benzyl-3,4,5-trimethyl-4H-pyrazole (23147-80-0) → syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.02,6>octane-3,5-dione (164321-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 14 percent / CH₂Cl₂ / 20 °C

2: CD₃CN / 0.17 h / -30 °C / Irradiation; various photolysis conditions mode, various reaction conditions

In dichloromethane; [D₃]acetonitrile;

DOI:10.1021/jo00107a007

Reference yield:

anti-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.02,6>octane-3,5-dione (164145-76-0) → syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.02,6>octane-3,5-dione (164321-96-4)

Guidance literature:

In [D₃]acetonitrile; at -30.1 ℃; Thermodynamic data; ΔG, ΔH, ΔS;

DOI:10.1021/jo00107a007

Reference yield:

anti-1,4,7,10-Tetramethyl-10-(phenylmethyl)-2,4,6,8,9-pentaazatricyclo<5.2.1.02,6>dec-8-ene-3,5-dione → syn-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.02,6>octane-3,5-dione (164321-96-4) + anti-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.02,6>octane-3,5-dione (164145-76-0)

Guidance literature:

In dichloromethane; at 0 ℃; for 1.16667h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;

DOI:10.1021/jo00107a007

upstream raw materials:

anti-1,4,7,8-Tetramethyl-8-(phenylmethyl)-2,4,6-triazatricyclo<5.1.0.0^2,6>octane-3,5-dione

4-benzyl-3,4,5-trimethyl-4H-pyrazole

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