C₆₀H₈₀N₄O₁₂SSi₂

Base Information

Chemical Name:C₆₀H₈₀N₄O₁₂SSi₂
CAS No.:1334176-57-6
Molecular Formula:C₆₀H₈₀N₄O₁₂SSi₂
Molecular Weight:1137.55
Hs Code.:

C<sub>60</sub>H<sub>80</sub>N<sub>4</sub>O<sub>12</sub>SSi<sub>2</sub>

Synonyms:C₆₀H₈₀N₄O₁₂SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₀H₈₀N₄O₁₂SSi₂

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Technology Process of C₆₀H₈₀N₄O₁₂SSi₂

There total 12 articles about C₆₀H₈₀N₄O₁₂SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1334176-56-5
C₆₆H₉₄N₄O₁₂SSi₃

: 1334176-57-6
C₆₀H₈₀N₄O₁₂SSi₂

Guidance literature:: With pyridinium p-toluenesulfonate; In methanol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201101821

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 1334176-57-6
C₆₀H₈₀N₄O₁₂SSi₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / acetonitrile / 4 h / -20 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 0 - 20 °C / Inert atmosphere

7.1: acetic anhydride; acetic acid / 50 h / 20 °C / Inert atmosphere

8.1: pyridinium p-toluenesulfonate / methanol / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; N-Bromosuccinimide; pyridinium p-toluenesulfonate; acetic anhydride; pyridine hydrogenfluoride; acetic acid; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201101821

Reference yield:

: 1334176-52-1
N⁽³⁾-benzyloxymethyl-3',5'-O-di(tert-butyldimethylsilyl)-5-bromomethyl-2'-deoxyuridine

: 1334176-57-6
C₆₀H₈₀N₄O₁₂SSi₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: pyridine hydrogenfluoride / acetonitrile / 4 h / -20 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 0 - 20 °C / Inert atmosphere

4.1: acetic anhydride; acetic acid / 50 h / 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / methanol / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; pyridinium p-toluenesulfonate; acetic anhydride; pyridine hydrogenfluoride; acetic acid; lithium diisopropyl amide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201101821