tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

Base Information

Chemical Name:tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate
CAS No.:1620145-02-9
Molecular Formula:C₃₆H₃₅N₃O₄
Molecular Weight:573.692
Hs Code.:

Synonyms:tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

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Technology Process of tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

There total 2 articles about tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 34943-91-4
1-benzyl-3-methyl-1,3-dihydro-2H-indol-2-one

: 1373942-84-7
tert-butyl (1-benzyl-2-oxoindolin-3-ylidene)carbamate

: 1620145-02-9
tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

Guidance literature:: With (DHQD)2PHAL; In tert-butyl methyl ether; at 10 ℃; for 24h; Reagent/catalyst; Solvent; Temperature; stereoselective reaction;
DOI:10.1039/c4ob01039f

Reference yield:

: 34943-91-4
1-benzyl-3-methyl-1,3-dihydro-2H-indol-2-one

: 1373942-84-7
tert-butyl (1-benzyl-2-oxoindolin-3-ylidene)carbamate

: 1620145-02-9
tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

: 1620145-26-7
tert-butyl (1,1'-dibenzyl-3'-methyl-2,2'-dioxo-[3,3'-biindolin]-3-yl)carbamate

Guidance literature:: With (DHQD)2PHAL; In tert-butyl methyl ether; at 20 ℃; for 24h; Reagent/catalyst; Solvent; Temperature; Overall yield = 90 %; stereoselective reaction;
DOI:10.1039/c4ob01039f